Antimony Refining Process

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Antimony and arsenic substance flow analysis in antimony

Table 3 Ratio of antimony loss from each process No. Process Antimony loss ratio/% 1 Pelletization <0.01 2 Volatilization smelting 2.05 3 Forehearth 1.59 4 Cupellation furnace 1.03 5 Dust collection 0.78 6 Reduction smelting 0.17 7 Refining 0.29 8 Casting <0.01 According to the mass-balance principle, the total input of the system is equal to ...

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Lead Refining Process

Lead Refining Process. The building is a lofty, well-ventilated one of hardwood frame, with galvanized-iron walls and roof, and consists of five spans running north and south, covering a total length of 230 ft. Each span is composed of nine bays of 13-ft. centres, making the total width of the building 117 ft. ... One 46-ton Antimony softener ...

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Energy-efficient fluorine-free electro-refining of crude lead …

Currently, the electro-refining process of crude lead employs fluosilicic acid (H 2 SiF 6) [10], fluoboric acid [11], perchloric acid [12] and alkaline system [13] — among which the H 2 SiF 6 system (Betts method) is the most mature and widely deployed [10].But the H 2 SiF 6-based lead electro-refining is suffering environmental burden.This is attributed to the high volatility of …

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Separation behavior of arsenic and lead from antimony …

During zone refining process, As concentration in the whole bar was considerably reduced from 456 ppm to below 150 ppm (and as low as 50 ppm at the end of the bar) after only one zone pass by adding 0.1 wt.% Al into the Sb, which is contributed to the floating of formed AlAs intermetallic. ... Method for removal of lead and arsenic in crude ...

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CN104328289A

Belonging to the technical field of non-ferrous metal smelting, the invention relates to a method for removal of lead and arsenic in a crude antimony vacuum refining process. The method includes: first of all, adding a metal additive accounting for 1%-5% of the mass of crude antimony to obtain a mixed material, with the metal additive being metal manganese, metal aluminum or a …

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antimony refining process

A small number of antimony ore flotation concentrator using a single process, most of the antimony ... and then by reduction smelting and refining, as the metal antimony. ASTM B237 - 01(2010) Standard Specification for Refined Antimony

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Lead and tin removal from antimony metal by refining …

and time regime. The reported research has resulted in the optimal composition for refining antimony to remove lead and tin. Under optimal refining conditions, has been received the refined antimony metal with the remaining lead and tin as low as 0.015-0.008% and 0.005-0.001% respectively. Key words: PRIMARY ANTIMONY METAL, REFINING, LEAD, OIL

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Impurity Distribution During Electrolytic Refining of Antimony

An electrolytic refining process is used in order to obtain antimony with an overall impurity content not above 0.1–0.3%. In this this case the complete scheme for comprehensive treatment of antimony raw material includes: flame refining of ferrous metal electrolysis in solutions, solution purification from accumulated impurities, and anode sludge treatment with …

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Bismuth Metallurgy

Fire-refining process is the main method for bismuth refining. Electrochemical refining process is used only for crude bismuth, which is difficult to be refined directly by fire-refining process. ... oxidation refining and alkaline refining for arsenic, antimony and tellurium removal, zinc-adding for silver removal, chlorination for zinc and ...

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ALTERNATIVE FLUXES FOR LEAD BULLION REFINING

The Harris process for lead softening uses sodium hydroxide and sodium nitrate to remove arsenic, tin, and antimony from molten lead by oxidation. It is known to be better than oxygen softening, however the process has a high cost in terms of reagent used. Sodium hydroxide is corrosive and expensive.

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